Batman avoids a public unmasking but is unable to bring in the Joker, thanks to the villain's utility belt. Eventually, Batman and Robin are captured by the Joker's gang. But the Joker doesn't know a showdown with the Dynamic Duo awaits.
Dr. Shivel aka Mr. Freeze has returned and is seeking revenge on Batman, who accidentally spilled a freeze solution on him, being forced to live in a -50 climate. He is committing crimes involving diamonds, or "ice," in different forms. He freezes the duo, who look like goners.
Jervis Tetsch, aka the Mad Hatter, is abducting all the jurors who convicted him of a previous crime wave. He is also taking their hats. His final target is none other than Batman, who provided the key testimony in the Mad Hatter's trial. Batman and Robin have the Mad Hatter and his gang cornered but the criminal mastermind manages to encase the Caped Crusader in plaster of Paris.
Batman, thanks to superior breath control, is able to escape the plaster of Paris in which he was encased. Despite this, the Mad Hatter is still at large. Eventually, Batman and Robin again face off against the Mad Hatter at his criminal lair. Things look bad, but the Dyamic Duo manage to triumph.
Alfred contacts Batman by radio from the Batcave. Batman instructs the butler to short circuit a communications device the hero has on his wrist. This enable Batman to get free of his bonds. He and Robin get free just before they would be run over by a subway train. The Dynamic Duo resume their pursuit of False Face, which ends up at an old movie studio.
Catwoman initiates a series of thefts that cause Commissioner Gordon to summon Batman and Robin. But the importance of the crimes go beyond the taking of the objects involved. The Dynamic Duo eventually find Catwoman's lair. But Robin is whisked away while Batman is given a choice between two doors. If he picks the right door, he'll find Catwoman. If he picks the wrong one, he'll face certain doom. The hero makes the wrong selection and is about to be attacked by a tiger.
Batman evades the attacking tiger thanks to his utility belt. First, he scales the wall. Then, he uses a sonic device "to split the tiger's skull," as narrator William Dozier informs us. The hero still has to free Robin, who is facing a separate death trap. Once that task is completed, the Dynamic Duo are back on Catwoman's trail. It turns out the feline villain is after the lost treasure of Captain Manx, which is in a remote spot outside of Gotham City.
Taking advantage of the Riddler's mistaken belief that they were killed escaping his deathtrap, the Dynamic Duo must stop the villain from stealing a treasure of Incan jewels that would mean destroying an archaeological treasure as well.
A former academic who thinks he is really King Tut has returned. Batman and Robin seek his capture. A twist occurs, however, when King Tut's gang kidnaps Bruce Wayne. They are taking the millionaire in an ambulance. As Bruce tries to get free, the rear doors of the ambulance open and Bruce rides a cart toward a cliff.
Bruce frees himself just before the cart he is riding goes over a cliff. As Batman, he works to bring King Tut to justice. But the hero is captured by King Tut instead. Batman is then tortured as King Tut drops a pebble on his head at a time. Robin works to track Batman in time.